Query: journal:(J. Labelled Cpd. Radiopharm.) title:(Preparation of 14-C-labelled 1,4-Dideoxy-1,4-imino-D-arabinitol\: Cyanosilylation of Cyclic Imines using KCN in a One-Pot Synthesis), Author: Lundt

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journal:(J. Labelled Cpd. Radiopharm.) title:(Preparation of 14-C-labelled 1,4-Dideoxy-1,4-imino-D-arabinitol\: Cyanosilylation of Cyclic Imines using KCN in a One-Pot Synthesis) Author: Lundt

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journal:(J AND Labelled AND Cpd AND Radiopharm.) AND title:(Preparation AND of AND 14-C-labelled AND 1,4-Dideoxy-1,4-imino-D-arabinitol\: AND Cyanosilylation AND of AND Cyclic AND Imines AND using AND KCN AND in AND a AND One-Pot AND Synthesis)

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1 Journal article

Preparation of 14-C-labelled 1,4-Dideoxy-1,4-imino-D-arabinitol: Cyanosilylation of Cyclic Imines using KCN in a One-Pot Synthesis

Lundt, Inge; Malle, Birgitte Mølholm; Foged, Christian; Valsborg, Jacob S.

J. Labelled Cpd. Radiopharm — 1999, Volume 42, pp. 1145-1159

A new method for C-C bond formation was developed based on in situ cyanosilylation of cyclic Schiff bases using KCN, TMSCl, KI and ZnI2. This method was used to prepare the potent -glucosidase inhibitor 1,4-dideoxy-1,4-imino-D-arabinitol 14-C labelled at C-5.Keywords: in situ cyanosilylation; 14-C

Year: 1999

Language: English

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2 Journal article

Preparation of14C-labelled 1,4-dideoxy-1,4-imino-D-arabinitol: cyanosilylation of cyclic imines using KCN in a one-pot synthesis 10.1002/(SICI)1099-1344(199912)42:12<1145::AID-JLCR268>3.0.CO;2-Y