Journal article
Acetalization of furfural with zeolites under benign reaction conditions
Acetalization is a viable method to protect carbonyl functionalities in organic compounds and offers apotential synthetic strategy for synthesizing derived chemicals. In this work, several families of commer-cial zeolites have been employed as solid acid catalysts in the acetalization of furfural to form furfuraldiethyl acetal at room temperature using ethanol as a renewable solvent.
Among the tested catalysts,H-USY (6) provided the highest catalytic activity (79% acetal yield), excellent selectivity and reusabilityin five consecutive reaction runs. Process parameters such as, e.g. reaction time, catalyst loading andapplicability of different lower alcohols were evaluated and optimized
Language: | English |
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Year: | 2014 |
Pages: | 233-236 |
ISSN: | 18734308 and 09205861 |
Types: | Journal article |
DOI: | 10.1016/j.cattod.2014.03.004 |
ORCIDs: | Riisager, Anders |