Journal article
High accuracy interface characterization of three phase material systems in three dimensions
Microstructures and Interfaces, Fuel Cells and Solid State Chemistry Division, Risø National Laboratory for Sustainable Energy, Technical University of Denmark1
Fuel Cells and Solid State Chemistry Division, Risø National Laboratory for Sustainable Energy, Technical University of Denmark2
Risø National Laboratory for Sustainable Energy, Technical University of Denmark3
Image Analysis and Computer Graphics, Department of Informatics and Mathematical Modeling, Technical University of Denmark4
Department of Informatics and Mathematical Modeling, Technical University of Denmark5
Quantification of interface properties such as two phase boundary area and triple phase boundary length is important in the characterization ofmanymaterial microstructures, in particular for solid oxide fuel cell electrodes. Three-dimensional images of these microstructures can be obtained by tomography schemes such as focused ion beam serial sectioning or micro-computed tomography.
We present a high accuracy method of calculating two phase surface areas and triple phase length of triple phase systems from subvoxel accuracy segmentations of constituent phases. The method performs a three phase polygonization of the interface boundaries which results in a non-manifold mesh of connected faces.
We show how the triple phase boundaries can be extracted as connected curve loops without branches. The accuracy of the method is analyzed by calculations on geometrical primitives
Language: | English |
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Year: | 2010 |
Pages: | 8168-8176 |
ISSN: | 18732755 and 03787753 |
Types: | Journal article |
DOI: | 10.1016/j.jpowsour.2010.06.083 |
ORCIDs: | Jørgensen, Peter Stanley , Hansen, Karin Vels , Larsen, Rasmus and Bowen, Jacob R. |