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Journal article

High accuracy interface characterization of three phase material systems in three dimensions

From

Microstructures and Interfaces, Fuel Cells and Solid State Chemistry Division, Risø National Laboratory for Sustainable Energy, Technical University of Denmark1

Fuel Cells and Solid State Chemistry Division, Risø National Laboratory for Sustainable Energy, Technical University of Denmark2

Risø National Laboratory for Sustainable Energy, Technical University of Denmark3

Image Analysis and Computer Graphics, Department of Informatics and Mathematical Modeling, Technical University of Denmark4

Department of Informatics and Mathematical Modeling, Technical University of Denmark5

Quantification of interface properties such as two phase boundary area and triple phase boundary length is important in the characterization ofmanymaterial microstructures, in particular for solid oxide fuel cell electrodes. Three-dimensional images of these microstructures can be obtained by tomography schemes such as focused ion beam serial sectioning or micro-computed tomography.

We present a high accuracy method of calculating two phase surface areas and triple phase length of triple phase systems from subvoxel accuracy segmentations of constituent phases. The method performs a three phase polygonization of the interface boundaries which results in a non-manifold mesh of connected faces.

We show how the triple phase boundaries can be extracted as connected curve loops without branches. The accuracy of the method is analyzed by calculations on geometrical primitives

Language: English
Year: 2010
Pages: 8168-8176
ISSN: 18732755 and 03787753
Types: Journal article
DOI: 10.1016/j.jpowsour.2010.06.083
ORCIDs: Jørgensen, Peter Stanley , Hansen, Karin Vels , Larsen, Rasmus and Bowen, Jacob R.

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