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Journal article · Conference paper

Hydrothermal synthesis, off-axis electron holography and magnetic properties of Fe3O4 nanoparticles

By Almeida, Trevor P.1; Muxworthy, Adrian R.1; Williams, Wyn2; Kasama, Takeshi3; Dunin-Borkowski, Rafal E.4

From

Imperial College London1

University of Edinburgh2

Center for Electron Nanoscopy, Technical University of Denmark3

Forschungszentrum Jülich GmbH4

The hydrothermal synthesis of Fe3O4 nanoparticles (NPs) (<50 nm) from mixed FeCl3 / FeCl2 precursor solution at pH ~ 12 has been confirmed using complementary characterisation techniques of transmission electron microscopy and X-ray diffractometry. Off-axis electron holography allowed for visualisation of their single domain (SD) nature, as well as inter-particle interactions, with the latter attributed to explain the pseudo-SD/multi-domain behaviour demonstrated by bulk magnetic measurements.

Language: English
Publisher: IOP Publishing
Year: 2014
Pages: 012062
Proceedings: Electron Microscopy and Analysis Group Conference
ISSN: 17426596 and 17426588
Types: Journal article and Conference paper
DOI: 10.1088/1742-6596/522/1/012062
ORCIDs: Kasama, Takeshi

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