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Book chapter

Grain centre mapping - 3DXRD measurements of average grain characteristics

In Strain and Dislocation Gradients From Diffraction — 2014
From

Department of Physics, Technical University of Denmark1

Neutrons and X-rays for Materials Physics, Department of Physics, Technical University of Denmark2

European Synchrotron Research Facility3

Department of Mechanical Engineering, Technical University of Denmark4

Materials and Surface Engineering, Department of Mechanical Engineering, Technical University of Denmark5

Three-Dimensional X-ray Diraction (3DXRD) Microscopy is a generic term covering a variety of dierent techniques for characterising the mi- crostructure within the bulk of polycrystalline materials. One strategy | namely grain centre mapping | enables fast measurements of the av- erage characteristics of each grain (such as their centre-of-mass positions, volumes, phases, orientations and/or elastic strain tensor components), while the exact locations of the grain boundaries are unknown.

In the present chapter a detailed description of the setup and software for both grain centre mapping and the closely related boxscan method is given. Both validation experiments and applications for in situ studies of microstructural changes during plastic deformation and crack growth are given. Finally an outlook with special emphasis on coupling the measured results with modelling is given.

Language: English
Publisher: World Scientific
Year: 2014
Journal subtitle: Spatially-resolved Local Structure and Defects
ISBN: 1908979623 , 1908979631 , 9781908979629 and 9781908979636
Types: Book chapter
ORCIDs: Oddershede, Jette , Schmidt, Søren and Winther, Grethe

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