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Journal article

Crystallization in Pd40Ni40P20 glass

By Jiang, Jianzhong1; Saksl, K.2; Nishiyama, N.; Inoue, A.

From

Department of Physics, Technical University of Denmark1

Technical University of Denmark2

Phase segregation and the effect of pressure on crystallization of bulk and ribbon Pd40Ni40P20 glasses have been studied by means of differential scanning calorimetry (DSC) and x-ray diffraction. The DSC measurements show only one glass transition event in the samples annealed at different temperatures in the supercooled liquid region.

Phase analyses reveal at least five crystalline phases crystallized from the glass: monoclinic; body-centered tetragonal; orthorhombic; Ni2Pd2P and fcc-(Ni,Pd) solid solution phases. In the pressure range from 0 to 4.2 GPa, the crystallization temperature increases with pressure having a slope of 11 K/GPa.

The eutectic crystallization reaction mode and crystalline phases formed are unchanged in the pressure range used. The enhancement of the crystallization temperature with increasing pressure in the glass can be explained by the suppression of atomic mobility.

Language: English
Publisher: American Institute of Physics
Year: 2002
Pages: 3651-3656
ISSN: 10897550 and 00218979
Types: Journal article
DOI: 10.1063/1.1505681

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