Journal article
Analysis of the equivalent indenter concept used to extract Young’s modulus from a nano-indentation test: some new insights into the Oliver–Pharr method
In this paper a thorough analysis of the equivalent indenter concept applied to nano-indentation is carried out, motivated by the fact that previous works in the field have not considered the requirement of a consistent relation between contact depth and projected contact area. Dimensional analysis is initially used to prove that the shape of the axisymmetric equivalent indenter can be regarded as a material property, provided that size-effects are negligible.
Subsequently, it is shown that such shape can effectively be employed to describe the nano-indentation unloading stage by means of Sneddon's elastic solution which is formally valid only for indentation into a flat surface. This allows for formulating the problem of extracting Young's modulus from the unloading curve as an optimization problem.
However, it is proved that the latter does not have a unique solution, due to the particular mathematical structure of the underlying equations; hence, additional constraints are needed to set restrictions on the admissible equivalent indenter shapes. An example of such constraint is hidden in some apparent inconsistencies of the well-known Oliver–Pharr method, which is demonstrated to be based on an equivalent conical indenter whose semi-apical angle depends on the ratio between residual and total penetration.
Specifically, this angle tends to 90° when the material exhibits extensive inelastic deformation, whereas it reduces to the one characteristic of the real indenter for a perfectly elastic material. This provides a new physical explanation for the relatively good accuracy of the method even in presence of a non-negligible residual contact impression on the sample.
Language: | English |
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Year: | 2017 |
Pages: | 045004 |
ISSN: | 1361651x and 09650393 |
Types: | Journal article |
DOI: | 10.1088/1361-651X/aa6831 |
ORCIDs: | Andriollo, Tito and Hattel, Jesper Henri |