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Journal article

Highly Selective Continuous Gas-Phase Methoxycarbonylation of Ethylene with Supported Ionic Liquid Phase (SILP) Catalysts

In Chemcatchem — 2017, Volume 9, Issue 10, pp. 1824-1829

By Khokarale, Santosh Govind1; Garcia Suárez, Eduardo José1,2,3; Fehrmann, Rasmus1,2,3; Riisager, Anders1,2,3

From

Centre for Catalysis and Sustainable Chemistry, Department of Chemistry, Technical University of Denmark1

Department of Chemistry, Technical University of Denmark2

Organic Chemistry, Department of Chemistry, Technical University of Denmark3

Supported ionic liquid phase (SILP) technology was applied for the first time to the Pd-catalyzed continuous, gas-phase methoxycarbonylation of ethylene to selectively produce methyl propanoate (MP) in high yields. The influence of catalyst and reaction parameters such as, for example, ionic liquid loading, metal concentration, and ligand loadings was studied, and in particular the SILP catalyst activity and stability was found to be strongly dependent on the ligand to metal ratio.

Language: English
Year: 2017
Pages: 1824-1829
ISSN: 18673899 and 18673880
Types: Journal article
DOI: 10.1002/cctc.201601428
ORCIDs: Garcia Suárez, Eduardo José , Fehrmann, Rasmus and Riisager, Anders
Keywords

carbonylation fixed-bed technology ionic liquids palladium supported ionic liquid phase catalysis

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