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Journal article

A laser heating facility for energy-dispersive X-ray absorption spectroscopy

From

Department of Physics, Technical University of Denmark1

Neutrons and X-rays for Materials Physics, Department of Physics, Technical University of Denmark2

European Synchrotron Radiation Facility3

A double-sided laser heating setup for diamond anvil cells installed on the ID24 beamline of the ESRF is presented here. The setup geometry is specially adopted for the needs of energy-dispersive X-ray absorption spectroscopic (XAS) studies of materials under extreme pressure and temperature conditions.

We illustrate the performance of the facility with a study on metallic nickel at 60 GPa. The XAS data provide the temperature of the melting onset and quantitative information on the structural parameters of the first coordination shell in the hot solid up to melting.

Language: English
Publisher: AIP Publishing
Year: 2018
Pages: 013111
ISSN: 10897623 and 00346748
Types: Journal article
DOI: 10.1063/1.5010345
ORCIDs: Kantor, Innokenty

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