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Journal article

Synthesis and single crystal X-ray analysis of two griseofulvin metabolites

In Tetrahedron Letters — 2010, Volume 51, Issue 45, pp. 5881-5882

By Rønnest, Mads Holger^1,2; Harris, Pernille^2,3; Gotfredsen, Charlotte Held^1,2; Larsen, T.O.; Clausen, Mads Hartvig^1,2

From

Organic Chemistry, Department of Chemistry, Technical University of Denmark¹

Department of Chemistry, Technical University of Denmark²

X-ray Crystallography, Department of Chemistry, Technical University of Denmark³

Abstract

The two phenols, 6-O-desmethyl griseofulvin and 4-O-desmethyl griseofulvin are metabolites of the antifungal drug griseofulvin. Herein, we present an improved synthesis of the 6-phenol derivative, and an unequivocal proof of both structures by single-crystal X-ray analysis.

Language:	English
Year:	2010
Pages:	5881-5882
ISSN:	18733581 and 00404039
Types:	Journal article
DOI:	10.1016/j.tetlet.2010.08.095
ORCIDs:	Harris, Pernille , Gotfredsen, Charlotte Held and Clausen, Mads Hartvig

Keywords

Griseofulvin Metabolites Synthesis X-ray structures

Synthesis and single crystal X-ray analysis of two griseofulvin metabolites

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Synthesis and single crystal X-ray analysis of two griseofulvin metabolites

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