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Journal article

Molecular structure of poly(3-alkyl-thiophenes) investigated by calorimetry and grazing incidence X-ray scattering

By Abad, Jose1,2; Espinosa, Nieves3; Ferrer, Pilar5,6; García-Valverde, Rafael3; Miguel, Carmen3; Padilla, Javier2; Alcolea, Alberto4; Castro, German R.5,6; Colchero, Jaime1; Urbina, Antonio3

From

Departamento de Física, Centro de Investigacion en Optica y Nanofisica, Universidad de Murcia, Campus de Espinardo, 30100 Murcia, Spain1

Departamento de Física Aplicada, Universidad Politécnica de Cartagena, Plaza del Hospital 1, 30202 Cartagena, Spain2

Departamento de Electrónica, Universidad Politécnica de Cartagena, Plaza del Hospital 1, 30202 Cartagena, Spain3

Servicio de Apoyo a la Investigación Tecnológica (SAIT), Universidad Politécnica de Cartagena, Plaza del Hospital 1, 30202 Cartagena, Spain4

SpLine, Spanish CRG beamline at the ESRFacility, 6 rue Jules Horowitz B.P, 38043 Grenoble, France5

Instituto de Ciencia de Materiales de Madrid, CSIC, calle Sor Juana Inés de la Cruz, 3, 28049 Madrid, Spain6

Highlights► In this work we study of the molecular structure of P3OT and P3HT and the phase transitions. ► From the calorimetric diagrams we obtain the melting and crystallization temperatures. ► We identify a low temperature calorimetric glass transition. ► GIXRD shows an increase of the crystallinity for the P3HT and not in the P3OT with the annealing. ► Interdigitation of the side chain is produced for the P3HT and not in the P3OT.

Language: English
Year: 2011
ISSN: 18793398 and 09270248
Types: Journal article
DOI: 10.1016/j.solmat.2011.09.025

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