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Conference paper

Heteronuclear long-range correlation, what’s new and how far can it take us?

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Department of Chemistry, Technical University of Denmark1

The lecture will give an overview of the references below with emphasis on the key features of the pulse sequences and the ideas behind them. Heteronuclear two-bond correlation: Suppressing heteronuclear three-bond or higher NMR correlations while enhancing two-bond correlations even for vanishing 2J(CH).

Nyberg NT, Duus JØ, Sørensen OW, JOURNAL OF THE AMERICAN CHEMICAL SOCIETY Volume: 127 Issue: 17 Pages: 6154-6155 Published: MAY 4 2005 Editing of H2BC NMR spectra. Nyberg NT, Duus JØ, Sørensen OW, MAGNETIC RESONANCE IN CHEMISTRY Volume: 43 Issue: 12 Pages: 971-974 Published: DEC 2005 H2BC: a new technique for NMR analysis of complex carbohydrates.

Petersen BO, Vinogradov E, Kay W, et al., CARBOHYDRATE RESEARCH Volume: 341 Issue: 4 Pages: 550-556 Published: MAR 20 2006 Improved multiplicity-editing of HMBC NMR spectra. Benie AJ, Sørensen OW, MAGNETIC RESONANCE IN CHEMISTRY Volume: 44 Issue: 8 Pages: 739-743 Published: AUG 2006 HAT HMBC: A hybrid of H2BC and HMBC overcoming shortcomings of both.

Benie AJ, Sørensen OW, JOURNAL OF MAGNETIC RESONANCE Volume: 184 Issue: 2 Pages: 315-321 Published: FEB 2007 Clean HMBC: Suppression of strong-coupling induced artifacts in HMBC spectra. Wurtz P, Permi P, Nielsen NC, et al., JOURNAL OF MAGNETIC RESONANCE Volume: 194 Issue: 1 Pages: 89-98 Published: SEP 2008 Adiabatic Low-Pass J Filters for Artifact Suppression in Heteronuclear NMR.

Meier S, Benie AJ, Duus JØ, et al., CHEMPHYSCHEM Volume: 10 Issue: 6 Pages: 893-895 Published: APR 14 2009 3D H2BC: A novel experiment for small-molecule and biomolecular NMR at natural isotopic abundance. Sebastian Meier, Andrew J. Benie, Jens Ø. Duus and Ole W. Sørensen, Journal of Magnetic Resonance, in press, doi:10.1016/j.jmr.2009.06.017 Recent progress in heteronuclear long-range NMR of complex carbohydrates: 3D H2BC and clean HMBC.

Sebastian Meier, Bent O. Petersen, Jens Ø. Duus, Ole W. Sørensen. Carbohydrate Research, in press, doi:10.1016/j.carres.2009.08.013

Language: English
Year: 2009
Proceedings: XXXIX National Congress on Magnetic Resonance
Types: Conference paper

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